HuagongsheHuagongshe Chemistry Print Report · For research reference only
Nicotinoyl chloride → HCID 59134180, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Nicotinoyl chloride | HCID 82604 | — |
| Reactant | 3-Amino-6-(4-chlorobenzyl)-1-(2,4-dichlorobenzenesulfonyl)-8-isopropylhexahydropyrazino[1,2-a]pyrimidine-4,7-dione | HCID 59134252 | — |
| Product | HCID 59134180 | HCID 59134180 | — |
Reaction Steps
Synthesis took place in analogy to Example 22 using nicotinoyl chloride *HCl and 3-amino-6-(4-chlorobenzyl)-1-(2,4-dichlorobenzenesulfonyl)-8-isopropyl-hexahydropyrazino[1,2-a]pyrimidine-4,7-dione. The desired product is obtained with MW=663.09 (calculated, monoisotopic); measured value (M+H)+: 664.11
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07652007B2 |
| Source dataset | uspto-grants-2010_01 |
| ORD ID | ord-4d738e0aac6349f5996b414380d89c0d |
| Source note | uspto-grants-2010_01 |