HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 54183701, compound → HCID 53828432, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 54183701 | HCID 54183701 | — |
| Reactant | HCID 178418546 | HCID 178418546 | — |
| Solvent | HCID 20488916 | HCID 20488916 | — |
| Product | HCID 53828432 | HCID 53828432 | 77.3% |
Reaction Steps
90.5 g of 1-ethylcyclopropanecarboxylic acid chloride is stirred in 100 ml of acetonitrile:trichloroethylene (1:1) with 79.3 g of CuCN for 12 hours at 80° C. The cooled suspension is filtered, the filtrate is evaporated to dryness and the residue is distilled to yield 65 g of colourless 1-ethylcyclopropylcarboxylic acid cyanide having a boiling point at 60 millibars of 88° C.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04402733 |
| Source dataset | uspto-grants-1983_09 |
| ORD ID | ord-47fbd3347df5401fa009bbb42cac0e28 |
| Source note | uspto-grants-1983_09 |