HuagongsheHuagongshe Chemistry Print Report · For research reference only
Iodoethane → HCID 178477462, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Iodoethane | HCID 6340 | — |
| Reactant | Diisopropyl Ether | HCID 7914 | — |
| Reactant | Ethyl Acetate | HCID 8857 | — |
| Reactant | HCID 12952717 | HCID 12952717 | — |
| Solvent | Acetic Acid | HCID 176 | — |
| Product | HCID 178477462 | HCID 178477462 | — |
Reaction Steps
A mixture of 17.3 parts of N-(2,2-dimethoxyethyl)-N'-[4-(4-methoxyphenyl)-1-piperazinyl]thiourea, 17 parts of iodoethane, 180 parts of ethyl acetate and 20 parts of acetic acid is stirred for 3 hours. Upon the addition of 2,2'-oxybispropane, the product is precipitated. It is filtered off and triturated in 4-methyl-2-pentanone. The product is filtered off and crystallized from 2-propanol, yielding 9 parts of ethyl N-(2,2-dimethoxyethyl)-N'-[4-(4-methoxyphenyl)-1-piperazinyl]carbamimidothioate monohydroiodide.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04402957 |
| Source dataset | uspto-grants-1983_09 |
| ORD ID | ord-19700fed3c6340b9b66a22794672c434 |
| Source note | uspto-grants-1983_09 |