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HRID1995288

反应详情

EQUATION

反应方程式

HRID 1995288 的结构方程式

REACTANTS

反应物

2
结构：Cl.ClCCN1CC2CCC(CC2)C1
HCID12612326

3-(2-Chloroethyl)-3-azabicyclo[3.2.2]nonane--hydrogen chloride (1/1)

C10H19Cl2N

结构：CC(C)(C)c1ccc2c3c(c(=O)oc2c1)CNCC3
HCID13136921

未命名化合物

PRODUCTS

生成物

1
结构：CC(C)(C)c1ccc2c3c(c(=O)oc2c1)CN(CCN1CC2CCC(CC2)C1)CC3.Cl.Cl
HCID13189012

未命名化合物

收率 48%

PROCEDURE

实验过程

Prepared by the method described for Example 1 from 8-(1,1-dimethylethyl)-1,2,3,4-tetrahydro-5H-[1]benzopyrano[3,4-c]-pyridin-5-one (4 g, 0.016 moles) and 3-(2-chloroethyl)-3-azabicyclo(3.2.2)nonane hydrochloride (3.6 g, 0.016 moles). Recrystallization from methanol gave the product (3.7 g), mp 312°-315° C.

WORKUP

后处理

  1. customPrepared by the method
  2. customRecrystallization from methanol