HCID 13219107, compound → HCID 53942627, compound

Participants

Reaction Steps

To 4.0 g of N,N'-bis[4-[(2,3,4,6-tetra-O-acetyl-β-D-glucopyranosyl)thio]phenyl]pentanediamide was added 500 ml of ammonia saturated methanol at 0° C. The solution was kept at 0° C. for 2 hours, then at ambient temperature overnight and taken to dryness in vacuo. The residue was triturated with 20 ml of absolute ethanol and the resulting solid was collected, giving 1.45 g of the desired intermediate as an amorphous solid.

Provenance & Evidence