HuagongsheHuagongshe Chemistry Print Report · For research reference only
3-Chloropyridine-2-carboxylic acid → HCID 178522734, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 3-Chloropyridine-2-carboxylic acid | HCID 824632 | — |
| Reactant | HCID 178509299 | HCID 178509299 | — |
| Solvent | Thionyl Chloride | HCID 24386 | — |
| Product | HCID 178522734 | HCID 178522734 | 39.3% |
Reaction Steps
0.53 g of 3-chloro-2-pyridinecarboxylic acid, 10 ml of thionyl chloride and 0.27 g of 5-aminotetrazole are treated in the same manner as described in Example 1. The crude product thus obtained is recrystallized from a mixture of dimethylformamide and ethanol, whereby 0.28 g of N-(5-tetrazolyl)-3-chloro-2-pyridinecarboxamide is obtained.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04404214 |
| Source dataset | uspto-grants-1983_09 |
| ORD ID | ord-506cde04188f4f70be64ab4491622625 |
| Source note | uspto-grants-1983_09 |