HRID1995359
反应详情
EQUATION
反应方程式
REACTANTS
反应物
PRODUCTS
生成物
AUXILIARIES
试剂、催化剂与溶剂
PROCEDURE
实验过程
0.94 g of 6-n-butoxy-2-pyridinecarboxylic acid, 10 ml of thionyl chloride and 0.48 g of 5-aminotetrazole are treated in the same manner as described in Example 1. The crude product thus obtained is recrystallized from a mixture of dimethylformamide, water and ethanol, whereby 0.77 g of N-(5-tetrazolyl)-6-n-butoxy-2-pyridinecarboxamide is obtained.
WORKUP
后处理
- customThe crude product thus obtained
- customis recrystallized from a mixture of dimethylformamide, water and ethanol