HuagongsheHuagongshe Chemistry Print Report · For research reference only
Thionyl Chloride → HCID 178428764, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Thionyl Chloride | HCID 24386 | — |
| Reactant | 6-methyl-4-nitropicolinic acid | HCID 11275391 | — |
| Reactant | HCID 178509299 | HCID 178509299 | — |
| Product | HCID 178428764 | HCID 178428764 | 40.1% |
Reaction Steps
1.44 g of 4-nitro-6-methyl-2-pyridinecarboxylic acid, 27 ml of thionyl chloride and 0.79 g of 5-aminotetrazole are treated in the same manner as described in Example 1. The crude product thus obtained is washed with ethanol, whereby 0.79 g of N-(5-tetrazolyl)-4-nitro-6-methyl-2-pyridinecarboxamide is obtained.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04404214 |
| Source dataset | uspto-grants-1983_09 |
| ORD ID | ord-65871b5624ae49da81f39eef8fbc239d |
| Source note | uspto-grants-1983_09 |