Tert-Butylamine → HCID 15567168, compound

Participants

Reaction Conditions

Reaction Steps

A solution of 7.3 gm (0.1 mol) of tert. butylamine in 20 ml of dioxane was added dropwise to a solution of 10.0 gm (42 mmols) of 3,5-dimethoxy-benzene sulfonic acid chloride in 100 ml dioxane at 40° C. over a period of 15 minutes. After the reaction temperature began to drop the reaction mixture was heated at 45° C. for 1.5 hours and at 60° C. for 2 hours. After cooling and filtering, the filtrate was evaporated in vacuo. The residue was recrystallized from cyclohexane.

Provenance & Evidence