HuagongsheHuagongshe Chemistry Print Report · For research reference only
2-Methyl-3-nitroanisole → 3-Methoxy-2-methylaniline
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 2-Methyl-3-nitroanisole | HCID 78554 | — |
| Reactant | HCID 178418361 | HCID 178418361 | — |
| Catalyst | Nickel | HCID 935 | — |
| Solvent | Ethanol | HCID 702 | — |
| Product | 3-Methoxy-2-methylaniline | HCID 11804822 | — |
Reaction Steps
200 gm (1.19 mols) of 2-methoxy-6-nitro-toluene were hydrogenated in 2.5 liters of ethanol in the presence of 25 gm of Raney nickel at 100 bar until the absorption of the calculated amount of hydrogen. The reaction mixture was filtered and evaporated in vacuo. After distillation 158.3 gm (97% of theory) of 3-methoxy-2-methylaniline were obtained.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04404230 |
| Source dataset | uspto-grants-1983_09 |
| ORD ID | ord-5afd0e1827d6400aaa1e43226f127dd0 |
| Source note | uspto-grants-1983_09 |