HuagongsheHuagongshe Chemistry Print Report · For research reference only
2(3H)-Benzoxazolone → HCID 18006576, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 2(3H)-Benzoxazolone | HCID 6043 | — |
| Reactant | Methylamine | HCID 6329 | — |
| Product | HCID 18006576 | HCID 18006576 | — |
Reaction Steps
Benzoxazolinone (1 mole) was stirred with 2 moles of methylamine (25% aqueous solution) for 48 hours at 50° C., then some of the water and the excess of methylamine were distilled off at 60° C. under reduced pressure. The desired urea crystallised out on cooling; it had m.pt. 130° C. (decomp.).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04404356 |
| Source dataset | uspto-grants-1983_09 |
| ORD ID | ord-fd488989e793443882b2f79670f72754 |
| Source note | uspto-grants-1983_09 |