HuagongsheHuagongshe Chemistry Print Report · For research reference only
2,6-Dichlorobenzoyl isocyanate → HCID 13242735, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 2,6-Dichlorobenzoyl isocyanate | HCID 12912739 | — |
| Reactant | 6-(4-Chlorophenyl)pyridin-3-amine | HCID 20402529 | — |
| Solvent | Acetonitrile | HCID 6342 | — |
| Product | HCID 13242735 | HCID 13242735 | — |
Reaction Steps
6-(4-Chlorophenyl)-3-pyridylamine (70 mg) was dissolved in 45 ml acetonitrile and treated with 2,6-dichlorobenzoyl isocyanate (0.25 gram) under nitrogen at room temperature. A precipitate formed almost immediately and after about 2 hours stirring, the solid was collected and recrystallized from ethanol, yield, 200 mg, m.p. 225°-229° C. The identity of the product was confirmed by NMR.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04405552 |
| Source dataset | uspto-grants-1983_09 |
| ORD ID | ord-c40d8515b2544969ba6d2dd5132e1a87 |
| Source note | uspto-grants-1983_09 |