HuagongsheHuagongshe Chemistry Print Report · For research reference only
Oxalic Acid → HCID 20471304, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Oxalic Acid | HCID 971 | — |
| Reactant | 1-[(3,4-Dimethylphenyl)methyl]-1H-imidazole | HCID 13045367 | — |
| Solvent | Ethanol | HCID 702 | — |
| Product | HCID 20471304 | HCID 20471304 | — |
Reaction Steps
A hot solution of oxalic acid (0.225 g,0.0025 mol) in dry ethanol (10 ml) was added to a solution of 1-(3,4-dimethylbenzyl)imidazole (0.46 g,0.0025 mol) in hot ethanol (20 ml). After boiling for 0.25 h, the solution was evaporated to afford a white solid. Recrystallisation of the solid from ethanol/petroleum ether (b.p. 40°-60°) afforded 1-(3,4-dimethylbenzyl)imidazole hydrogen oxalate as a white solid, m.p. 92°-93°.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04405634 |
| Source dataset | uspto-grants-1983_09 |
| ORD ID | ord-01feb0faac0d4b00ab18d1c54d371785 |
| Source note | uspto-grants-1983_09 |