Diglycidyl ether → HCID 20487811, compound

HRID 1995729Notes

Reaction equation

HRID 1995729 reaction equation
[CH3:1][C:2]1([CH3:11])[CH2:7][CH:6]([OH:8])[CH2:5][C:4]([CH3:10])([CH3:9])[NH:3]1.[O:12]1[CH2:20][CH:13]1[CH2:14][O:15][CH2:16][CH:17]1[O:19][CH2:18]1>C(O)C>[OH:12][CH:13]([CH2:20][N:3]1[C:4]([CH3:9])([CH3:10])[CH2:5][CH:6]([OH:8])[CH2:7][C:2]1([CH3:11])[CH3:1])[CH2:14][O:15][CH2:16][CH:17]([OH:19])[CH2:18][N:3]1[C:4]([CH3:10])([CH3:9])[CH2:5][CH:6]([OH:8])[CH2:7][C:2]1([CH3:11])[CH3:1]

Participants

4

Reactant 2

HCID 16704Diglycidyl etherHCID 754714-Hydroxy-2,2,6,6-tetramethylpiperidine

Product 1

HCID 20487811HCID 20487811, compound

Reagents, catalysts & solvents 1

HCID 702EthanolSolvent

Procedure

2,2,6,6-Tetramethyl-4-hydroxypiperidine 15.7 g and bis(2,3-epoxypropyl)ether was dissolved in 30 ml ethanol and refluxed for ten hours. Ethanol was distilled off, and 21.8 g of colorless liquid was obtained.

Workup

  1. temperaturerefluxed for ten hours
  2. distillationEthanol was distilled off

Sources & evidence

ORD record
ord-6c9f8048ab904c6382335b1a034244ad
Source dataset
uspto-grants-1983_09
Patent number
US04405737

Reaction notes

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