HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 1995769Generated: October 30, 2026
Formaldehyde → N-methyl-N-tertiarybutylaminoethoxyethanol
https://huagongshe.com/reaction/1995769
Participants
| Role | Name | HCID | Charge |
|---|
| Reactant | Formaldehyde | HCID 712 | — |
| Reactant | Tertiarybutylaminoethoxyethanol | HCID 86739037 | — |
| Catalyst | Palladium | HCID 23938 | — |
| Solvent | Methanol | HCID 887 | — |
| Product | N-methyl-N-tertiarybutylaminoethoxyethanol | HCID 86739036 | 81.2% |
Reaction Steps
A total of 145 g of tertiarybutylaminoethoxyethanol, 108 g of 37% aqueous formaldehyde, 10 g of 10% Pd/C, and 1 l of methanol were charged to an autoclave, pressured up to 1000 psi with H2 and heated at 80° C. for 8 hours. Filtration and distillation of the reaction mixture yielded 128 g of N-methyl-N-tertiarybutylaminoethoxyethanol with b.p. of 128° C. at 23 mm.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|
| Patent number | US04405811 |
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| Source dataset | uspto-grants-1983_09 |
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| ORD ID | ord-fe697eead4f6480caab9e00afd11fee4 |
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| Source note | uspto-grants-1983_09 |
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