3-Chloro-2-methyl-1-propene → HCID 12648299, compound
Reaction equation
[CH2:1]([C:8]([CH2:10][CH3:11])=[O:9])[C:2]1[CH:7]=[CH:6][CH:5]=[CH:4][CH:3]=1.[CH3:12][C:13]([CH2:15]Cl)=[CH2:14]>>[CH3:14][C:13]([CH2:15][CH:1]([C:2]1[CH:7]=[CH:6][CH:5]=[CH:4][CH:3]=1)[C:8](=[O:9])[CH2:10][CH3:11])=[CH2:12]Participants
3
Procedure
If ethyl benzyl ketone is reacted with β-methallyl chloride according to the foregoing details, then there is obtained 2-methyl-4-phenyl-hept-1-en-5-one of boiling point 93° C./3 mmHg; nD20 =1.5094.
Sources & evidence
- ORD record
- ord-b7fb55c3389d4d68a634c32deee08858
- Source dataset
- uspto-grants-1983_09
- Patent number
- US04406828
Reaction notes
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