HuagongsheHuagongshe Chemistry Print Report · For research reference only
Phenylacetone → HCID 539743, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Phenylacetone | HCID 7678 | — |
| Reactant | 3-Chloro-1-butene | HCID 11242 | — |
| Reactant | Crotyl chloride | HCID 11589 | — |
| Product | HCID 539743 | HCID 539743 | — |
Reaction Steps
Methyl benzyl ketone is reacted with crotyl chloride or 3-chloro-1-butene in accordance with the foregoing details and there is obtained 5-phenyl-hept-2-en-6-one of boiling point 88° C./3 mmHg; nD20 =1.5190. When 3-chloro-1-butene is used there is also obtained 3-methyl-5-phenyl-hex-1-en-5-one which is separated by distillation.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04406828 |
| Source dataset | uspto-grants-1983_09 |
| ORD ID | ord-8181b469060444e5acd91dfe58543465 |
| Source note | uspto-grants-1983_09 |