Methylhydrazine → HCID 13229057, compound

Participants

Reaction Steps

1.71 ml of methylhydrazine dissolved in 30 ml of methanol are added to a stirred solution of 4-methoxy-1-methyl-6-phenyl-1,2-dihydro-1,3,5-triazin-2-one in 100 ml of methanol. The mixture is stirred for one hour at RT and then refluxed for four hours. The reaction mixture is concentrated and the triazinone precipitated from ethyl acetate and hexane, filtered, washed with ether, and dried to yield 1.95 g of the desired product.

Provenance & Evidence