Formamide → HCID 178479553, compound

HRID 1995906Notes

Reaction equation

HRID 1995906 reaction equation
[CH:1]([NH2:3])=[O:2].[CH2:4]([Cl:11])[C:5]1[CH:10]=[CH:9][CH:8]=[CH:7][CH:6]=1>>[ClH:11].[CH2:4]([C:1](=[NH:3])[OH:2])[C:5]1[CH:10]=[CH:9][CH:8]=[CH:7][CH:6]=1

Participants

3

Reactant 2

HCID 713FormamideHCID 7503Benzyl Chloride

Product 1

HCID 178479553HCID 178479553, compound

Procedure

The product was assayed by NMR δ (DMSO) 5.7 (s, 2H, φCH2), 7.5 (s, 5H, φ), 9.0 (s, 1H HC=N). The product is thermally unstable. It decomposes to formamide and benzyl chloride at 0° C. and above. However, no appreciable decomposition was detected on storage at -20° C. for 2 months.

Workup

  1. waitHowever, no appreciable decomposition was detected on storage at -20° C. for 2 months

Sources & evidence

ORD record
ord-8971d6c55a4e440ab9ea35ed201e9704
Source dataset
uspto-grants-1983_09
Patent number
US04406902

Reaction notes

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