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HRID20030

反应详情

EQUATION

反应方程式

HRID 20030 的结构方程式

REACTANTS

反应物

2
结构：Clc1csc(Cl)n1
HCID12333155

2,4-Dichloro-1,3-thiazole

C3HCl2NS

结构：COC(=O)[C@@H](CI)C(=O)OC(C)(C)C
HCID86614124

未命名化合物

PRODUCTS

生成物

1
结构：COC(=O)[C@H](Cc1nc(Cl)cs1)C(=O)OC(C)(C)C
HCID67305732

未命名化合物

PROCEDURE

实验过程

The title compound was synthesized in a manner analogous to that described Example 475, using (R)-methyl 2-(tert-butoxycarbonyl)-3-iodopropanoate and 2,4-dichlorothiazole (prepared according to Reynaud, Pierre; Robba, Max; Moreau, Robert C; New synthesis of the thiazole ring; Bulletin de la Societe Chimique de France (1962), 1735-8). MS m/z: 321 (23%, M+1), 265.0 (100%, M−55.1).

WORKUP

后处理

  1. customprepared
  2. customNew synthesis of the thiazole ring