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HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 2022258Generated: October 31, 2026

Di-tert-butyl bicarbamate → HCID 178428597, compound

https://huagongshe.com/reaction/2022258

Reaction equation

Participants

RoleNameHCIDCharge
ReactantDi-tert-butyl bicarbamateHCID 85431—
Reactant2-Bromo-4-methylpyridineHCID 2734087—
ReagentLithium HexamethyldisilazideHCID 2733832—
Catalystpalladium(II) acetateHCID 167845—
CatalystBinap, (A+-)-HCID 634876—
Solvent1,4-DioxaneHCID 31275—
ProductHCID 178428597HCID 178428597—
Internal standard9-PhenylanthraceneHCID 11766—

Reaction Conditions

Temperature110 °C

Provenance & Evidence

DOI10.1038/s41557
Source dataset39k HTE dataset from Pfizer
ORD IDord-f6a688c6623f48efacbf2664e822046e
Source note39k HTE dataset from Pfizer