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HRID2025

反应详情

EQUATION

反应方程式

HRID 2025 的结构方程式

REACTANTS

反应物

2
结构：CCCn1cnc2c1c(=O)[nH]c(=O)n2C
HCID3314397

3-Methyl-7-propylxanthine

C9H12N4O2

结构：CCOP(=O)(CCCCCl)OCC
HCID19689195

未命名化合物

PRODUCTS

生成物

1
结构：CCCn1cnc2c1c(=O)n(CCCCP(=O)(OCC)OCC)c(=O)n2C
HCID22446293

未命名化合物

PROCEDURE

实验过程

The title substance was prepared from 0.072 mol of 3-methyl-7-propyl-xanthine and 0.072 mol of diethyl 4-chlorobutanephosphonate analogously to Example 23, chromatographed on silica gel (eluent: dichloromethane/methanol 20:1) and crystallized from diisopropyl ether.

WORKUP

后处理

  1. customchromatographed on silica gel (eluent: dichloromethane/methanol 20:1)
  2. customcrystallized from diisopropyl ether