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HRID2028

反应详情

EQUATION

反应方程式

HRID 2028 的结构方程式

REACTANTS

反应物

2
结构：CCOP(=O)(CCCBr)OCC
HCID283500

Diethyl(3-bromopropyl)phosphonate

C7H16BrO3P

结构：CCOCn1cnc2c1c(=O)[nH]c(=O)n2C
HCID13747684

未命名化合物

PRODUCTS

生成物

1
结构：CCOCn1cnc2c1c(=O)n(CCCP(=O)(OCC)OCC)c(=O)n2C
HCID22446302

未命名化合物

PROCEDURE

实验过程

The title substance was prepared from 0.048 mol of 7-ethoxymethyl-3-methylxanthine and 0.058 mol of diethyl 3-bromopropanephosphonate analogously to Example 32 and chromatographed on silica gel (eluent: ethyl acetate/methanol 10:1).

WORKUP

后处理

  1. customchromatographed on silica gel (eluent: ethyl acetate/methanol 10:1)