Cyclopropanemethanamine → HCID 58450729, compound

HRID 2035535Notes

Reaction equation

HRID 2035535 reaction equation
[CH2:1]([O:3][C:4]([C:6]1[CH:7]=[N:8][C:9]([Cl:13])=[CH:10][C:11]=1Cl)=[O:5])[CH3:2].[CH:14]1([CH2:17][NH2:18])[CH2:16][CH2:15]1>>[CH2:1]([O:3][C:4]([C:6]1[CH:7]=[N:8][C:9]([Cl:13])=[CH:10][C:11]=1[NH:18][CH2:17][CH:14]1[CH2:16][CH2:15]1)=[O:5])[CH3:2]

Participants

3

Reactant 2

HCID 75646CyclopropanemethanamineHCID 600045Ethyl 4,6-dichloropyridine-3-carboxylate

Product 1

HCID 58450729HCID 58450729, compound

Procedure

From 4,6-dichloropyridine-3-carboxylic acid ethyl ester synthesized according to the method described in US2006/0217417 and cyclopropylmethylamine in a manner similar to Example 339, the title compound was obtained as a slight yellow crystalline powder (yield 77%).

Sources & evidence

ORD record
ord-41a04fb6c55f44449da657ff32e6385d
Source dataset
uspto-grants-2013_11
Patent number
US08575153B2

Reaction notes

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