HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 76577160, compound → HCID 57828218, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 76577160 | HCID 76577160 | — |
| Catalyst | Palladium | HCID 23938 | — |
| Solvent | Ethanol | HCID 702 | — |
| Product | HCID 57828218 | HCID 57828218 | 89.4% |
Reaction Steps
{3-[4-(4-Azido-but-1-enyl)-naphthalen-1-yloxy]-propyl}-carbamic acid tert-butyl ester 3.5 g was hydrogenated in ethanol with 5% Pd/C (50% wet) for 2 h. Catalyst was removed, and the filtrate was concentrated to give 2.94 g of {3-[4-(4-Amino-butyl)-naphthalen-1-yloxy]-propyl}-carbamic acid tert-butyl ester.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08575176B2 |
| Source dataset | uspto-grants-2013_11 |
| ORD ID | ord-8f5249614845413d8146ee0b673702aa |
| Source note | uspto-grants-2013_11 |