HuagongsheHuagongshe Chemistry Print Report · For research reference only
(5-Fluoropyridin-3-yl)boronic acid → HCID 67433428, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | (5-Fluoropyridin-3-yl)boronic acid | HCID 44717403 | — |
| Reactant | HCID 67430914 | HCID 67430914 | — |
| Product | HCID 67433428 | HCID 67433428 | — |
Reaction Steps
Prepared according to Step C3b in General Procedure C using (S)-methyl 2-(1-(benzyloxycarbonylamino)ethyl)-3-iodoimidazo[1,2-a]pyridine-5-carboxylate (0.350 g, 0.730 mmol) and 5-fluoropyridin-3-ylboronic acid (0.154 g, 1.10 mmol) to give (S)-methyl 2-(1-(benzyloxycarbonylamino)ethyl)-3-(5-fluoropyridin-3-yl)imidazo[1,2-a]pyridine-5-carboxylate as a tan solid. LC-MS (ESI) m/z 449.1 [M+H]+.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08575183B2 |
| Source dataset | uspto-grants-2013_11 |
| ORD ID | ord-a87f7cb9a838444eae57d5bf7f97834e |
| Source note | uspto-grants-2013_11 |