(3-Chlorophenyl)boronic acid → HCID 25182134, compound

Participants

Reaction Steps

The title compound was prepared following procedures analogous to those in Example 56 using 3-(4-chloropyrimidin-2-yl)-6-methyl-6-phenyl-1,3-oxazinan-2-one and 3-chlorophenylboronic acid. LC-MS Method 3, tR=1.354 min, m/z=781.1. 1H NMR (CDCl3) 1.80 (s, 3H), 2.48-2.53 (m, 1H), 2.62-2.71 (m, 1H), 3.55-3.67 (m, 1H), 4.30-4.40 (m, 1H), 7.30-7.60 (m, 8H), 7.90-7.95 (m, 1H), 8.05 (s, 1H), 8.80-8.85 (m, 1H).

Provenance & Evidence