HuagongsheHuagongshe Chemistry Print Report · For research reference only
Methyl iodide → 4-Bromo-5,6-dimethylpyridin-2-ol
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Methyl iodide | HCID 6328 | — |
| Reactant | Potassium Carbonate | HCID 11430 | — |
| Reactant | 4-Bromo-5,6-dimethylpyridin-2-ol | HCID 46916251 | — |
| Product | 4-Bromo-5,6-dimethylpyridin-2-ol | HCID 46916251 | — |
| Product | HCID 66736202 | HCID 66736202 | — |
Reaction Steps
4-bromo-1,5,6-trimethylpyridin-2(1H)-one was prepared by alkylation of 4-bromo-5,6-dimethylpyridin-2(1H)-one with methyl iodide using K2CO3 following a procedure analogous to that described in Example 628 Step 1. 4-bromo-5,6-dimethylpyridin-2(1H)-one was prepared following the procedure described in McElroy, W. T. and DeShong, P. Org. Lett. 2003, 5, 4779.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08575156B2 |
| Source dataset | uspto-grants-2013_11 |
| ORD ID | ord-6e182b04c6b24588b4170a0d35c752ee |
| Source note | uspto-grants-2013_11 |