HuagongsheHuagongshe Chemistry Print Report · For research reference only
2,4-Dibromo-1-(2-bromoethoxy)benzene → HCID 11563691, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 2,4-Dibromo-1-(2-bromoethoxy)benzene | HCID 12725188 | — |
| Reactant | 1-Azabicyclo[2.2.2]oct-4-yl(diphenyl)methanol | HCID 23992385 | — |
| Solvent | Acetonitrile | HCID 6342 | — |
| Product | HCID 11563691 | HCID 11563691 | 52.6% |
Reaction Steps
Following the general procedure outlined in Example 4, 1-azabicyclo[2.2.2]oct -4-yl(diphenyl)methanol (0.0557 g, 0.190 mmol) and 2-bromoethyl 2,4-dibromophenyl ether (0.110 g, 0.306 mmol) in 2 CH3CN/3CHCl3 (4.0 mL) were reacted to give the desired product (0.0525 g, 43.8%). ELMS m/z 572(M+) Rt (2.26 min).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08575347B2 |
| Source dataset | uspto-grants-2013_11 |
| ORD ID | ord-c1fe96460c6c47d1b7ebebc0062c7631 |
| Source note | uspto-grants-2013_11 |