HuagongsheHuagongshe Chemistry Print Report · For research reference only
Benzene, (2-bromoethoxy)- → HCID 11569697, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Benzene, (2-bromoethoxy)- | HCID 68526 | — |
| Reactant | HCID 68963321 | HCID 68963321 | — |
| Solvent | Acetonitrile | HCID 6342 | — |
| Product | HCID 11569697 | HCID 11569697 | 54.5% |
Reaction Steps
Following the general procedure outlined in Example 4, 1-azabicyclo[2.2.2]oct -4-yl(di-3-thienyl)methanol (0.0787 g, 0.258 mmol) and 2-bromoethyl phenyl ether (0.0839 g, 0.417 mmol) in 2MeOH/3CHCl3/2 CH3CN (5.0 mL) were reacted to give the desired product (0.0709 g, 54.5%). EI-MS m/z 426(M+) Rt (1.85 min).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08575347B2 |
| Source dataset | uspto-grants-2013_11 |
| ORD ID | ord-f36f129d88e0444c88da8b7ea395dacd |
| Source note | uspto-grants-2013_11 |