HuagongsheHuagongshe Chemistry Print Report · For research reference only
Benzene, (3-bromopropoxy)- → HCID 11591704, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Benzene, (3-bromopropoxy)- | HCID 68522 | — |
| Reactant | HCID 68963321 | HCID 68963321 | — |
| Solvent | Acetonitrile | HCID 6342 | — |
| Product | HCID 11591704 | HCID 11591704 | 44.7% |
Reaction Steps
Following the general procedure outlined in Example 4, 1-azabicyclo[2.2.2]oct -4-yl(di-3-thienyl)methanol (0.0808 g, 0.264 mmol) and 3-bromopropyl phenyl ether (0.070 mL, 0.444 mmol) in 2MeOH/3CHCl3/2 CH3CN (5.0 mL) were reacted to give the desired product (0.0613 g, 44.7%). ELMS m/z 440(M+) Rt (2.05 min).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08575347B2 |
| Source dataset | uspto-grants-2013_11 |
| ORD ID | ord-d21f100923a340448ed57026023ce6bd |
| Source note | uspto-grants-2013_11 |