HuagongsheHuagongshe Chemistry Print Report · For research reference only
Allyl bromide → HCID 11495315, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Allyl bromide | HCID 7841 | — |
| Reactant | 1-Azabicyclo[2.2.2]oct-4-yl(diphenyl)methanol | HCID 23992385 | — |
| Solvent | Acetonitrile | HCID 6342 | — |
| Product | HCID 11495315 | HCID 11495315 | 79.8% |
Reaction Steps
Following the general procedure outlined in Example 3, 1-azabicyclo[2.2.2]oct -4-yl(diphenyl)methanol (0.0577 g, 0.197 mmol) and 3-bromo-1-propene (0.025 mL, 0.289 mmol) in 2 CH3CN/3CHCl3 (4.0 mL) were reacted to give the desired product (0.0646 g, 79.8%). ELMS m/z 334(M+) Rt (1.54 min).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08575347B2 |
| Source dataset | uspto-grants-2013_11 |
| ORD ID | ord-c080495d9b094e9eba8dc60f5adce37e |
| Source note | uspto-grants-2013_11 |