HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 43823076, compound → HCID 67042601, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 43823076 | HCID 43823076 | — |
| Solvent | Acetic Anhydride | HCID 7918 | — |
| Product | HCID 67042601 | HCID 67042601 | 81% |
Reaction Steps
A stirred solution of 2-{[(4-nitrophenyl)acetyl]amino}benzoic acid (7.5 g, 25 mmol) in acetic anhydride (50 mL) was refluxed for 3 hours. The solvent was removed in vacuum and the residue was taken up in diethyl ether, to provide after filtration and drying the title compound (5.7 g, 81% yield).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08580783B2 |
| Source dataset | uspto-grants-2013_11 |
| ORD ID | ord-9b42b5c9b8084d6880637f06367f89e0 |
| Source note | uspto-grants-2013_11 |