Isopropylamine → HCID 57855967, compound

Participants

Reaction Steps

See step f) of example H2 for the reaction conditions starting from 9-chloro-2-[2-(3-chloro-pyridin-2-yl)-5-trifluoromethyl-2H-pyrazol-3-yl]-6,7-dimethyl-3-oxa-1,5,8-triaza-anthracen-4-one and 2 equivalents of isopropylamine. After 18 hours reaction time and purification by flash chromatography on silica gel, a white solid is obtained within 42% yield. m.p.: 243-244° C.

Provenance & Evidence