HuagongsheHuagongshe Chemistry Print Report · For research reference only
Ammonia → 2-phenyl-4H,5H,6H,7H-(1,3)thiazolo(5,4-c)pyridine
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Ammonia | HCID 222 | — |
| Reactant | Thiobenzamide | HCID 683563 | — |
| Solvent | Dimethylformamide | HCID 6228 | — |
| Product | 2-phenyl-4H,5H,6H,7H-(1,3)thiazolo(5,4-c)pyridine | HCID 22337487 | — |
Reaction Steps
4.5 g of the product of step a) are charged to a round-bottomed flask with 34 ml of DMF and 2.6 g of thiobenzamide. Heating is carried out at a temperature of 60° C. for 6 hours. An aqueous ammonia solution is added until a basic pH is obtained and evaporation is carried out under vacuum.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08580790B2 |
| Source dataset | uspto-grants-2013_11 |
| ORD ID | ord-32c591e910204d8788cbb6653c2cc3d7 |
| Source note | uspto-grants-2013_11 |