HuagongsheHuagongshe Chemistry Print Report · For research reference only
2-(3-Aminophenyl)ethan-1-ol → HCID 58327696, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 2-(3-Aminophenyl)ethan-1-ol | HCID 14938987 | — |
| Reactant | HCID 58961526 | HCID 58961526 | — |
| Product | HCID 58327696 | HCID 58327696 | — |
Reaction Steps
(4-((3-(2-Hydroxyethyl)phenyl)amino)-7H-pyrrolo[2,3-d]pyrimidin-5-yl)(phenyl)methanone was synthesized using 2-(3-aminophenyl)ethanol and (4-chloro-7H-pyrrolo[2,3-d]pyrimidin-5-yl)(phenyl)methanone according to the general procedure A. A white solid was obtained. M.p.>300° C.; 400 MHz 1HNMR (DMSO-d6) δ 11.25 (s, 1H), 8.42 (s, 1H), 7.90-7.81 (m, 4H), 7.65-7.55 (m, 4H), 7.26 (m, 1H), 6.90 (d, J=7.2 Hz, 1H), 4.63 (s, 1H), 3.61-3.60 (m, 2H), 2.74-2.70 (m, 2H); LCMS [M+H] 359.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08580803B2 |
| Source dataset | uspto-grants-2013_11 |
| ORD ID | ord-2d320e945a70409f9fcb8ba371ca64e9 |
| Source note | uspto-grants-2013_11 |