HuagongsheHuagongshe Chemistry Print Report · For research reference only
m-Aminoacetanilide → HCID 58327720, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | m-Aminoacetanilide | HCID 7604 | — |
| Reactant | HCID 86654847 | HCID 86654847 | — |
| Product | HCID 58327720 | HCID 58327720 | — |
Reaction Steps
N-(3-((5-(2-Methylbenzo yl)-7H-pyrrolo[2,3-d]pyrimidin-4-yl)amino)phenyl)acetamide was synthesized using N-(3-aminophenyl)acetamide and ((4-chloro-7H-pyrrolo[2,3-d]pyrimidin-5-yl)(o-tolyl)methanone according to the general procedure A. An off-white solid was obtained. M.p.>300° C.; 400 MHz 1HNMR (DMSO-d6) δ 11.36 (s, 1H), 10.01 (s, 1H), 8.46 (s, 1H), 8.06 (s, 1H), 7.73 (d, J=7.6 Hz, 1H), 7.57 (s, 1H), 7.49-7.45 (m, 2H), 7.39-7.28 (m, 4H), 2.34 (s, 3H), 2.02 (s, 3H); LCMS [M+H] 386.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08580803B2 |
| Source dataset | uspto-grants-2013_11 |
| ORD ID | ord-707d73c5754d43c69fb715818cc6cf69 |
| Source note | uspto-grants-2013_11 |