3-Amino-N-methylbenzamide → HCID 58327745, compound

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Reaction Steps

3-((5-(1-Naphthoyl)-7H-pyrrolo[2,3-d]pyrimidin-4-yl)amino)-N-methylbenzamide was synthesized using 3-amino-N-methylbenzamide and (4-chloro-7H-pyrrolo[2,3-d]pyrimidin-5-yl)(naphthalen-1-yl)methanone according to the general procedure A. A yellow solid was obtained. M.p.>300° C.; 400 MHz 1HNMR (DMSO-d6) δ 11.53 (s, 1H), 8.48-8.44 (m, 2H), 8.24-8.20 (m, 2H), 8.14 (d, J=8.0 Hz, 1H), 8.06-8.03 (m, 2H), 7.80-7.78 (m, 1H), 7.70 (d, J=2.4 Hz, 1H), 7.64-7.53 (m, 3H), 7.50-7.44 (m, 2H), 2.77 (d, J=4.4 Hz, 3H); LCMS [M+H] 422.

Provenance & Evidence