HuagongsheHuagongshe Chemistry Print Report · For research reference only
m-Aminoacetanilide → HCID 58327718, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | m-Aminoacetanilide | HCID 7604 | — |
| Reactant | HCID 86654848 | HCID 86654848 | — |
| Product | HCID 58327718 | HCID 58327718 | — |
Reaction Steps
N-(3-((5-(1-Naphthoyl)-7H-pyrrolo[2,3-d]pyrimidin-4-yl)amino)phenyl)acetamide was synthesized using N-(3-aminophenyl)acetamide and (4-chloro-7H-pyrrolo[2,3-d]pyrimidin-5-yl)(naphthalen-1-yl)methanone according to the general procedure A. A yellow solid was obtained. M.p.>300° C.; 400 MHz 1HNMR (DMSO-d6) δ 11.42 (s, 1H), 9.98 (s, 1H), 8.45 (s, 1H), 8.13 (d, J=8.4 Hz, 1H), 8.05-8.02 (m, 3H), 7.79-7.73 (m, 2H), 7.67 (s, 1H), 7.63-7.53 (m, 4H), 7.38-7.35 (m, 1H), 7.29-7.25 (m, 1H), 2.02 (s, 3H); LCMS [M+H] 422.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08580803B2 |
| Source dataset | uspto-grants-2013_11 |
| ORD ID | ord-24e112fcba154a5fb24a00c2d38accf0 |
| Source note | uspto-grants-2013_11 |