HuagongsheHuagongshe Chemistry Print Report · For research reference only
Hydrochloric Acid → HCID 44159023, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Hydrochloric Acid | HCID 313 | — |
| Reactant | HCID 66922239 | HCID 66922239 | — |
| Reactant | HCID 66922373 | HCID 66922373 | — |
| Product | HCID 44159023 | HCID 44159023 | 98.7% |
Reaction Steps
The compound of step 6 (27.0 mg, 48.2 μmol) was reacted analogously as described in example 1, step 7. Dissolution of the obtained solid in a small quantity of MOH, addition of hydrochloric acid (0.1 M) and lyophilization overnight yielded 21.9 mg of the title compound in the form of [2-(5-fluoro-2-methyl-phenoxy)-1-phenyl-1H-pyrrolo[2,3-c]pyridin-3-yl]-piperazin-1-yl-methanone dihydrochloride.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08580813B2 |
| Source dataset | uspto-grants-2013_11 |
| ORD ID | ord-a636abe77c3249f29ecc2f0ef63ec528 |
| Source note | uspto-grants-2013_11 |