HuagongsheHuagongshe Chemistry Print Report · For research reference only
Hydrochloric Acid → HCID 66922245, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Hydrochloric Acid | HCID 313 | — |
| Reactant | HCID 66922124 | HCID 66922124 | — |
| Reactant | HCID 66922396 | HCID 66922396 | — |
| Product | HCID 66922245 | HCID 66922245 | 82.8% |
Reaction Steps
The compound of step 6 (30.0 mg, 53.5 μmol) was reacted analogously as described in example 1, step 7. Dissolution of the obtained solid in a small quantity of MOH, addition of hydrochloric acid (0.1 M) and lyophilization overnight yielded 20.4 mg of the title compound in the form of the [2-(5-fluoro-2-methyl-phenoxy)-5-methoxy-1-phenyl-1H-pyrrolo[2,3-b]pyridin-3-yl]-piperazin-1-yl-methanone dihydrochloride.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08580813B2 |
| Source dataset | uspto-grants-2013_11 |
| ORD ID | ord-6646ee9403c74b188afe45dccf63cc24 |
| Source note | uspto-grants-2013_11 |