HCID 66922399, compound → HCID 66922329, compound

HRID 2039851Notes

Reaction equation

HRID 2039851 reaction equation
Cl[C:2]1[CH:7]=[CH:6][N:5]=[C:4]2[N:8]([C:11]3[CH:16]=[CH:15][CH:14]=[CH:13][CH:12]=3)[CH:9]=[CH:10][C:3]=12.[CH2:17]([Mg]Cl)[CH2:18][CH3:19]>>[C:11]1([N:8]2[C:4]3=[N:5][CH:6]=[CH:7][C:2]([CH2:17][CH2:18][CH3:19])=[C:3]3[CH:10]=[CH:9]2)[CH:16]=[CH:15][CH:14]=[CH:13][CH:12]=1

Participants

3

Reactant 2

HCID 66922399HCID 66922399, compoundHCID 178455855HCID 178455855, compound

Product 1

HCID 66922329HCID 66922329, compound

Procedure

The title compound was prepared from the compound of step 1 (4.69 g, 20.5 mmol) and propylmagnesium chloride analogously as described in example 42, step 1. Yield: 3.57 g.

Sources & evidence

ORD record
ord-97b54911b6de49278df45df0b2458469
Source dataset
uspto-grants-2013_11
Patent number
US08580813B2

Reaction notes

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