2,6-Dimethylphenol → HCID 66922257, compound

HRID 2039870Notes

Reaction equation

HRID 2039870 reaction equation
[C:1]([O:5][C:6]([N:8]1[CH2:13][CH2:12][N:11]([C:14]([C:16]2[C:20]3=[N:21][CH:22]=[CH:23][CH:24]=[C:19]3[N:18]([C:25]3[CH:30]=[CH:29][CH:28]=[CH:27][CH:26]=3)[C:17]=2Cl)=[O:15])[CH2:10][CH:9]1[CH2:32][C:33]([O:35][CH3:36])=[O:34])=[O:7])([CH3:4])([CH3:3])[CH3:2].[CH3:37][C:38]1[CH:43]=[CH:42][CH:41]=[C:40]([CH3:44])[C:39]=1[OH:45]>>[C:1]([O:5][C:6]([N:8]1[CH2:13][CH2:12][N:11]([C:14]([C:16]2[C:20]3=[N:21][CH:22]=[CH:23][CH:24]=[C:19]3[N:18]([C:25]3[CH:30]=[CH:29][CH:28]=[CH:27][CH:26]=3)[C:17]=2[O:45][C:39]2[C:40]([CH3:44])=[CH:41][CH:42]=[CH:43][C:38]=2[CH3:37])=[O:15])[CH2:10][CH:9]1[CH2:32][C:33]([O:35][CH3:36])=[O:34])=[O:7])([CH3:4])([CH3:3])[CH3:2]

Participants

3

Reactant 2

HCID 113352,6-DimethylphenolHCID 66922233HCID 66922233, compound

Product 1

HCID 66922257HCID 66922257, compound

Procedure

The compound of step 1 (254 mg, 507 μmol) and 2,6-dimethylphenol were reacted analogously as described in example 1, step 6. 340 mg of crude title compound were obtained.

Sources & evidence

ORD record
ord-05bb114a324d47be8f5b6eae954ea584
Source dataset
uspto-grants-2013_11
Patent number
US08580813B2

Reaction notes

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