Triacetoxyperiodinane → HCID 87562064, compound

Participants

Reaction Steps

A reactor is charged with 150 mg (0.42 mmol) of the solid obtained in step 1 and 216 mg (0.5 mmol) of the Dess-Martin reagent in 5 ml acetonitrile. The mixture is stirred at room temperature for 16 hours. The insoluble compounds are filtered and the filtrate is concentrated under reduced pressure. The obtained solid is washed with ethylic ether and pentane to give the required aldehyde (120 mg, 82%).

Provenance & Evidence