HuagongsheHuagongshe Chemistry Print Report · For research reference only
3-Fluoro-4-hydroxybenzaldehyde → 4-(2-Fluoro-4-formyl-phenoxy)-naphthalene-1-carbonitrile
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 3-Fluoro-4-hydroxybenzaldehyde | HCID 587250 | — |
| Reactant | 1-Cyano-4-fluoronaphthalene | HCID 2736734 | — |
| Product | 4-(2-Fluoro-4-formyl-phenoxy)-naphthalene-1-carbonitrile | HCID 86623141 | — |
Reaction Steps
4-(2-Fluoro-4-formyl-phenoxy)-naphthalene-1-carbonitrile was prepared from 3-Fluoro-4-hydroxybenzaldehyde and 4-Fluoro-naphthalene-1-carbonitrile following General Procedure A. 1H NMR (400 MHz, CDCl3) δ 9.99 (d, J=1.95 Hz, 1H), 8.38 (d, J=8.6 Hz, 1H), 8.27 (d, J=8.6 Hz, 1H), 7.77-7.84 (3H), 7.69-7.74 (2H), 7.29 (d, J=7.43 Hz, 1H), 6.83 (d, J=7.83 Hz, 1H).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08580832B2 |
| Source dataset | uspto-grants-2013_11 |
| ORD ID | ord-97469de574ac418f9c2a6b6f66063008 |
| Source note | uspto-grants-2013_11 |