HuagongsheHuagongshe Chemistry Print Report · For research reference only
tert-Butyldimethylsilyl chloride → HCID 59676139, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | tert-Butyldimethylsilyl chloride | HCID 28928 | — |
| Reactant | HCID 44411867 | HCID 44411867 | — |
| Product | HCID 59676139 | HCID 59676139 | — |
Reaction Steps
Following the procedure described in Example 80, using 11-methyl-6,11-dihydro-5-thia-11-aza-benzo[a]fluoren-8-ol (1.15 g, 3.123 mmol) and TBSCl (562 mg, 3.75 mmol) as the starting material, the title compound was prepared as a white solid.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08580840B2 |
| Source dataset | uspto-grants-2013_11 |
| ORD ID | ord-3761c33bdd8c407795cf347b8c8c7226 |
| Source note | uspto-grants-2013_11 |