4-Hydroxy-2-Methoxybenzaldehyde → HCID 178493425, compound
Reaction equation
[OH:1][C:2]1C=CC(C=O)=C(OC)C=1.Cl[C:13]1[CH:14]=[C:15]([CH:20]=[C:21](OC)[C:22]=1[OH:23])[C:16]([NH:18][OH:19])=[NH:17]>>[OH:23][C:22]1[CH:13]=[CH:14][C:15]([C:16]([NH:18][OH:19])=[NH:17])=[C:20]([O:1][CH3:2])[CH:21]=1Participants
3
Procedure
The title compound is prepared form commercially available 4-hydroxy-2-methoxy-benzaldehyde in analogy to 3-chloro-4,N-dihydroxy-5-methoxy-benzamidine; LC-MS: tR=0.42 min; [M+1]+=183.04.
Sources & evidence
- ORD record
- ord-6980f718d96b4f4fa69911e132a133c3
- Source dataset
- uspto-grants-2013_11
- Patent number
- US08580824B2
Reaction notes
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