HuagongsheHuagongshe Chemistry Print Report · For research reference only
3-(3-Chlorophenyl)-2-propynal → 3-(3-Chlorophenyl)prop-2-ynal oxime
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 3-(3-Chlorophenyl)-2-propynal | HCID 46872540 | — |
| Reactant | 3-Phenylprop-2-ynal oxime | HCID 76543055 | — |
| Product | 3-(3-Chlorophenyl)prop-2-ynal oxime | HCID 76543056 | 96.4% |
Reaction Steps
The title compound was prepared following the method here described for Compound 1a, using Compound 31d instead of phenylpropiolaldehyde. The pale brown residue was used in the next step without further purification. Yield: 96.4%.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08580962B2 |
| Source dataset | uspto-grants-2013_11 |
| ORD ID | ord-a3b51d3f27f14f879e822be58fb81423 |
| Source note | uspto-grants-2013_11 |