3-(m-Tolyl)propiolaldehyde → N-hydroxy-3-(3-methylphenyl)prop-2-yn-1-imine

HRID 2040888Notes

Reaction equation

HRID 2040888 reaction equation
Cl[C:2]1[CH:3]=[C:4]([C:8]#[C:9][CH:10]=[N:11][OH:12])[CH:5]=[CH:6][CH:7]=1.[CH3:13]C1C=C(C#CC=O)C=CC=1>>[OH:12][N:11]=[CH:10][C:9]#[C:8][C:4]1[CH:5]=[CH:6][CH:7]=[C:2]([CH3:13])[CH:3]=1

Participants

3

Reactant 2

HCID 107731013-(m-Tolyl)propiolaldehydeHCID 765430563-(3-Chlorophenyl)prop-2-ynal oxime

Product 1

HCID 86662876N-hydroxy-3-(3-methylphenyl)prop-2-yn-1-imine

Procedure

The title compound was synthesized following the procedure reported for Compound 31e but starting from Compound 91b instead of Compound 31d. The crude title compound (brownish oil) was used in the next step without further purification.

Workup

  1. customThe crude title compound (brownish oil) was used in the next step without further purification

Sources & evidence

ORD record
ord-740331082d32413fb3a8b9f2ace8b25a
Source dataset
uspto-grants-2013_11
Patent number
US08580962B2

Reaction notes

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