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HRID2040906

反应详情

EQUATION

反应方程式

HRID 2040906 的结构方程式

REACTANTS

反应物

2
结构：NC(=O)N1CCC2(CC(C#Cc3cccc(Cl)c3)=NO2)C1
HCID56644646

未命名化合物

结构：Clc1cccc(C#CC2=NOC3(CCNC3)C2)c1
HCID57493822

未命名化合物

PRODUCTS

生成物

1
结构：NC(=O)N1CCC2(CC1)CC(C#Cc1cccc(Cl)c1)=NO2
HCID57493792

未命名化合物

PROCEDURE

实验过程

The title compound was synthesized following the method herein described for the compound of Example 96 but replacing Compound 22c for Compound 27d. After the usual work-up procedure the crude was purified by means of automated flash chromatography (Isolera®TM-Biotage; gradient Petroleum Ether-EtOAc from 1:0 to 93:7) giving the title compound as a white solid. Yield: 76.9%.

WORKUP

后处理

  1. customThe title compound was synthesized
  2. customAfter the usual work-up procedure the crude was purified by means of automated flash chromatography (Isolera®TM-Biotage; gradient Petroleum Ether-EtOAc from 1:0 to 93:7)